搜索 - 科创

%7B%22c%22%3A%22%E5%8F%A0%E6%B0%AE%E7%94%B2%E9%85%B0%E8%83%BA%22%2C%22t%22%3A%22%22%2C%22d%22%3A%22%22%2C%22selectedForums%22%3A%5B%5D%2C%22excludedForums%22%3A%5B%5D%2C%22threadCategories%22%3A%5B%7B%22_id%22%3A21%2C%22name%22%3A%22%E5%8C%85%E5%90%AB%E4%BA%BA%E5%B7%A5%E6%99%BA%E8%83%BD%E4%BA%A7%E7%89%A9%22%2C%22nodeName%22%3A%22%E4%B8%8D%E5%8C%85%E5%90%ABAI%E5%86%85%E5%AE%B9%22%2C%22nodes%22%3A%5B%7B%22_id%22%3A22%2C%22name%22%3A%22%E5%8C%85%E5%90%ABAI%E7%94%9F%E6%88%90%E7%9A%84%E9%87%8E%E7%94%9F%E5%86%85%E5%AE%B9%22%7D%2C%7B%22_id%22%3A24%2C%22name%22%3A%22%E4%BD%9C%E8%80%85%E5%AF%B9AI%E7%94%9F%E6%88%90%E5%86%85%E5%AE%B9%E8%B4%9F%E8%B4%A3%22%7D%2C%7B%22_id%22%3A23%2C%22name%22%3A%22%E4%BD%9C%E8%80%85%E8%B4%9F%E8%B4%A3%E3%80%81AI%E5%8D%8F%E5%8A%A9%22%7D%5D%7D%2C%7B%22_id%22%3A1%2C%22name%22%3A%22%E7%89%B9%E6%AE%8A%E8%AF%9D%E9%A2%98%22%2C%22nodeName%22%3A%22%E4%BB%A5%E4%B8%8A%E9%83%BD%E4%B8%8D%E6%98%AF%22%2C%22nodes%22%3A%5B%7B%22_id%22%3A2%2C%22name%22%3A%22%E6%8F%90%E9%97%AE%2F%E6%B1%82%E5%8A%A9%22%7D%2C%7B%22_id%22%3A13%2C%22name%22%3A%22%E6%97%B6%E4%BA%8B%E6%97%B6%E6%94%BF%22%7D%2C%7B%22_id%22%3A8%2C%22name%22%3A%22%E4%BA%8B%E6%95%85%E6%8A%A5%E5%91%8A%22%7D%5D%7D%2C%7B%22_id%22%3A5%2C%22name%22%3A%22%E5%8A%A8%E6%89%8B%E5%AE%9E%E8%B7%B5%22%2C%22nodeName%22%3A%22%E4%BB%A5%E4%B8%8A%E9%83%BD%E4%B8%8D%E6%98%AF%22%2C%22nodes%22%3A%5B%7B%22_id%22%3A6%2C%22name%22%3A%22%E5%AE%9E%E9%AA%8C%E6%8A%A5%E5%AF%BC%22%7D%2C%7B%22_id%22%3A7%2C%22name%22%3A%22%E7%A4%BE%E4%BC%9A%E5%AE%9E%E8%B7%B5%22%7D%5D%7D%2C%7B%22_id%22%3A9%2C%22name%22%3A%22%E4%B8%A5%E8%82%83%E5%86%85%E5%AE%B9%22%2C%22nodeName%22%3A%22%E4%BB%A5%E4%B8%8A%E9%83%BD%E4%B8%8D%E6%98%AF%22%2C%22nodes%22%3A%5B%7B%22_id%22%3A10%2C%22name%22%3A%22%E9%A2%84%E5%8D%B0%E6%9C%AC%22%7D%2C%7B%22_id%22%3A14%2C%22name%22%3A%22%E4%B8%93%E8%91%97%2F%E8%AE%BA%E8%BF%B0%22%7D%2C%7B%22_id%22%3A12%2C%22name%22%3A%22%E6%95%99%E7%A8%8B%2F%E8%AF%BE%E7%A8%8B%22%7D%2C%7B%22_id%22%3A11%2C%22name%22%3A%22%E4%B8%93%E4%B8%9A%E7%A7%91%E6%99%AE%22%7D%2C%7B%22_id%22%3A15%2C%22name%22%3A%22%E6%A0%87%E5%87%86%2F%E8%A7%84%E8%8C%83%22%7D%5D%7D%5D%2C%22form%22%3A%22%22%7D

H2SO4⒊使用光亮铁片作电极，将硝基脲溶解于含氯化铵与盐酸的溶液中通电电解（文献）NH2CONHNO2+H2SO4+3H2O——>NH2CONHNH2•H2SO4+3/2O2⒋硫酸氨基脲与亚硝酸钠反应得叠氮甲酰胺

很多文献都指出肼基与亚硝酸的反应选择性大于氨基和亚硝酸，只要亚硝酸不过量应该是没什么问题的，你可以自己去搜关键词，通过本文所阐述的方法制备叠氮甲酰胺同样有文献提及，不应该这么多篇文献都存在数据造假，作者过阵子会实践这个方法

nitrous acid on semicarbazides RNHCONHNH2（R=H,alkyl,or arya),carbamoyl azides have been prepared.还直接提到了叠氮甲酰胺已通过在低温下用亚硝酸钠处理盐酸氨基脲得到

文件下载

加载中...

你在 {{ downloadTime }} 下载过当前文件。

文件名称：{{ resource.defaultFile.name }}

下载次数：{{ resource.hits }}

上传用户：{{ uploader.username }}

所需积分：{{ costScores }}，{{ holdScores }}下载当前附件免费{{ description }}

下载地址：{{ l.name }}

积分不足，去充值

文件已丢失

当前账号的附件下载数量限制如下：

时段	个数
{{f.startingTime}}点 - {{f.endTime}}点	{{f.fileCount}}

约找到 4 条结果，耗时 0.143 秒

当前账号的附件下载数量限制如下：