搜索 - 科创

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在合成中的作用　　由于芳基重氮氟硼酸盐（ArN2BF4）可由芳香胺（ArNH2）经重氮化反应制得，该反应提供了一条由氨基（-NH2）引入氟原子（-F）的途径。　　

不知道加碱淬灭反应时有没有氨味，没有描述），又是不明价态的铜（没有粗略的表征，哪怕加酸看看溶不溶也可以），然后复杂价态的氮（不能确定有叠氮和铵根）统一被氧化成氮气不一定能计算叠氮根的产率，并且拍照或描述实验现象也不容易看（像重氮化的现象

em…我等级太低私信没法回你我的NaNT就是一步法无铜盐催化搞的 NaNO2溶液为底液升温到70℃然后缓慢滴入稀硫酸和氨基四唑的混合液 NaNO2和硫酸按理论投料比加就好了不要过量理论投料比重氮化反应已经进行的很完全了

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