搜索 - 科创网

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内容：刚刚查了下，锑度百科在碘的词条里制备这个部分上竟然写了一堆碘量法的内容.............so查了下维基，表示貌似海带提碘法这货是18-19世纪的老古董...维基上还注明此法不具有经济可行性现在主要的制碘方法是

内容：以便于制定改进方案或者进行下一步实验溶液配置:pH3.6缓冲液:将4mL冰乙酸与1.69g三水合乙酸钠于烧杯混合并加入少量水溶解,转移至50mL容量瓶,洗涤烧杯并将洗涤液转移至容量瓶,定容,摇匀,装瓶第一次实验:使用碘量法实验原理,如抗坏血酸.抗坏血酸能被碘定量氧化,可以用来滴定,但其较易被空气氧化.2.在使用硫代硫酸钠滴定前,调pH至3.5-4.0.可以通过加入缓冲液并稀释实现.第一次实验失败此处参考文献大多是中文第二次实验:使用碘量法实验原理

内容：1.原理使用间接碘量法测定Cu2+的反应方程式为2Cu2++4I-=====2CuI(沉淀)+I2I2+2S2O32-=====S4O62-+2I-铜离子与碘离子的反应是可逆的，为了使反应更加的完全，必须加入过量的

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