老外做的扫描电镜
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Cool Customer To keep the microscope’s vacuum pump from overheating, Krasnow used an air conditioner from a liquid-nitrogen generator he had built previously
Cody Pickens

Ben Krasnow has built his share of odd contraptions, including a liquid nitrogen generator made from an air conditioner, and the “thirst extinguisher,” a commercial-grade fire extinguisher that cools, carbonates, and dispenses his homemade beer. Now, for no other reason than wanting a real challenge, the 28-year-old engineer picked the toughest DIY project he could imagine: a homemade scanning electron microscope, or SEM. “I wanted to see if it was possible,” he says.
Scientific labs will pay upward of $250,000 for a high-end SEM, and as far as Krasnow could find, no individual had ever built one, so he had to improvise. He first spent a few weeks teaching himself the complex physics behind the instrument. Next he trolled eBay for cheap components, sorted through his home shop for power sources that might work, and then built what he couldn’t find.
A typical SEM fires a thin stream of electrons at a sample, monitors the electrons kicked up by the impact, and translates the resulting signals into a picture.

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Show Your Gold: The image of a necklace scanned by Krasnow’s microscope appears on the oscilloscope’s screen
Courtesy Ben Krasnow

Krasnow made his electron gun out of a thin tungsten wire. He heats up the wire by applying a voltage, which releases clouds of electrons. The freed electrons speed through a thin copper pipe toward the sample.
In his initial tests, Krasnow had trouble aiming the electron beam onto the sample. Eventually he took a refrigerator magnet and moved it around the outside of the glass vacuum chamber that surrounds the microscope to adjust the beam’s position. When he got the beam focused in the right place, he taped the magnet in place.
The microscope now delivers about 50x magnification, a far cry from commercial SEMs’ 1,000x or more, but microscope experts say that doesn’t lessen the accomplishment. Chemist Robert Wolkow of the University of Alberta calls it “a wonderful achievement.” And William Beaty, a research engineer and hobbyist who had also hoped to build the first DIY SEM, puts it more simply: “D’oh!”

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Under Glass: The bell jar that houses the microscope’s component
Cody Pickens

How It Works
Time: 100 hours
Cost: $1,500
Display
The SEM gets its name because the electron beam scans the surface of the sample; the resulting image is basically a video of a still subject. To create that video, Krasnow bought an old oscilloscope. As the beam moves across the surface, the clouds of electrons emitted from the sample change, and the oscilloscope transforms this physical data into a video image. The catch with the oscilloscope is that Krasnow scans the image in 1/15 of a second to get a picture, and quicker scans result in lower-resolution images. He plans to digitize the system and replace the oscilloscope with a computer, which should allow him to scan slowly and increase the microscope’s magnification.
Vacuum Cooling
To maintain the microscope’s thin beam of electrons, Krasnow had to eliminate any interference, so he housed the entire device in a large glass bell jar he had lying around. He used two separate pumps to create a vacuum inside the jar. One of the two has a tendency to overheat, so an aquarium pump sends engine coolant past the overheating pump, drawing out the heat, and cycles the fluid through a repurposed window-unit air conditioner, where it is cooled down before repeating the trip.
Retro Style
The oscilloscope and two of the power supplies look as if they could have been salvaged from a 1960s space mission. Krasnow liked the aesthetic, so he enclosed the power supplies in a similar-colored rack, arranged the other components above them, bought blank gray faceplates, drilled the necessary holes, and mounted chrome toggle switches, red indicator lights, knobs and gauges that matched the style.
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白天白
11年6个月前 IP:未同步
478973
[s:222]谁能翻译一下,第一句就难倒我了Cool Customer?
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tonghuamy
11年6个月前 IP:未同步
478982
我英文也不好,我在google在线翻译了一下,将就看吧,如下:

酷客户要保持显微镜的真空泵过热,Krasnow从一个液态氮发生器他已经建成以前科迪皮肯斯本Krasnow已建成自己的份额奇怪的玩意儿,包括一个液体氮气发生器由空调使用空调,并“干渴灭火器,”一个商业级的灭火器冷却,碳酸盐和分配他自制的啤酒。现在,没有别的原因,想要一个真正的挑战,28岁的工程师选择了最艰难的DIY项目,他可以想像:一个自制的扫描电子显微镜或扫描电子显微镜。 “我想看看,如果有可能,”他说。科学实验室将支付超过25万美元的高端扫描电镜,尽可能Krasnow能找到的,没有人在这么短的时间内建成一个,所以他只好凑合。他先花了几个星期自学复杂的物理仪器后面。接着,他又受控易趣廉价的组件,排序的电源可能通过他的家居店,然后建立他找不到的东西。一个典型的扫描电镜的电子触发的细流的采样,监测电子踢的影响,所产生的信号转换成图片。

显示你的黄金:一条项链Krasnow显微镜扫描的图像显示在示波器的屏幕上
礼貌本Krasnow

Krasnow他的电子枪的细钨丝。他加热丝通过施加一个电压,该发行的电子云的。通过薄铜管朝向样品释放出的电子速度。
在他最初的测试中,Krasnow瞄准的电子束在样品上遇到了麻烦。最终,他把一台冰箱磁铁周围的外侧的玻璃围绕显微镜的真空室中,调整光束的位置和移动。当他得到的光束聚焦在正确的地方,他用带子把磁铁的地方。
现在的显微镜提供约50倍的放大倍率,商业中小型企业的1000 x或更多的相距甚远,但显微镜专家说,不减少的成就。阿尔伯塔大学的的化学家罗伯特Wolkow的要求是“一个美妙的成就。”威廉·贝蒂,谁也希望打造的首款DIY SEM研究工程师和爱好者,把它更简单地说:“D'哦!”

在玻璃钟罩,里面显微镜的组成部分
科迪·皮肯斯

它如何工作
时间:100小时
费用:$ 1,500
显示
SEM得到它的名字,因为电子束扫描的苏【9127】ce的样品,产生的图像基本上是一个视频的问题。要创建的视频,Krasnow买了一辆旧的示波器。随着电子束在整个苏中移动【9127】CE,云样的变化发出的电子,示波器该物理数据转换成视频图像。与示波器的渔获物,Krasnow在1/15的第二次得到的图片扫描图像,更快的扫描结果在较低分辨率的图像。他计划数字化系统,并更换了一台电脑,示波器,应该让他慢慢来扫描和提高显微镜的放大倍率。
真空冷却
为了保持显微镜的细的电子束,Krasnow,以消除任何干扰,所以他住在一个大玻璃钟罩,他已经躺在整个设备。他用两个单独的泵里面的jar创造一个真空。其中的两个有过热倾向,这样一个水族馆泵将发动机冷却液过去的过热泵,画出来的热量,循环的流体通过改变用途的窗口单位的空调,它是冷却后再重复行。
复古风格
示波器和两个电源供应器,看起来好像他们可能已被打捞从20世纪60年代的太空任务。 Krasnow喜欢的审美,所以他附上了一个类似色的机架中的电源,安排他们上面的其他组成部分,买了空白的灰色面板,钻出所需的孔,并安装了镀铬的切换开关,红色指示灯,旋钮和仪表匹配的风格。
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daxus
11年6个月前 IP:未同步
478991
Cool Customer 从前后文看,应该是 “保温桶” ,猜测就是照片上的哥们右手边上那个有点像食堂装饭的保温桶。

第一句话:
保温桶用于防止电镜的升压器过热,Krasnow用了一个制液氮的空调机来完成它。。。。
不好翻译,但应该比google翻译的好理解了[s:178]
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改装pcp
11年6个月前 IP:未同步
479062
显微镜扫描的图像显示在示波器的屏幕上[s:271]
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